2 results about "Mixed solution" patented technology

The invention relates to a method for preparing a lithium iron phosphate / carbon composite material of a lithium ion battery, which belongs to the technical field of lithium ion batteries. The method for preparing the lithium iron phosphate / carbon composite material of the lithium ion battery comprises the following steps of: 1) preparing a suspending graphene-dispersed aqueous solution system, namely, crushing graphite to 1 to 5 microns, adding the crushed graphite into distilled water or purified water, adding 0.1 to 5 percent of surfactant, heating with stirring the mixed solution to 180 to 250 DEG C in a sealing way, performing stirring for 2 to 6 hours and reducing the temperature; 2) crushing lithium iron phosphate to the particle size of 1 to 5 microns, adding the crushed lithium iron phosphate into the distilled water or the purified water, adding with stirring 0.01 to 1 percent of coupling agent, performing uniform stirring, adding the graphene-dispersed aqueous solution, and performing stirring and filtration; and 3) vacuum-drying solid powder obtained by the filtration, and calcinating the dried solid powder for 2 to 12 hours to obtain the graphene-coated lithium iron phosphate cathode material. The method has the advantages of simple process, high material performance, high conductivity, high bulk density, high compacted density and the like.

The invention discloses a preparation method of 17[alpha]-hydroxyprogesterone, wherein the preparation method comprises the steps: refining: step 1, dissolving 1 W of a crude product into a mixed solution of 4-5 V dichloromethane and 6-8 V ethanol, and heating to dissolve the crude product; step 2, weighing activated carbon exceeding a preset amount, then putting the activated carbon into a drying device for drying, controlling the drying temperature to be 60-85 DEG C, and controlling the drying time to be 10-15 minutes; and step 3, taking out the activated carbon dried in the step 2, and then placing the activated carbon in a grinding device for fine grinding. According to the scheme, activated carbon in the refining process in an original scheme is finely processed and then added, so that the reaction rate is effectively increased, the time of reflux decoloration is shortened, large-scale production and processing are facilitated, and the production cost is further reduced.